{"note":{"id":"nte_9et4irv40d","attempt_id":"att_9wgv0fyay0","author_user_id":"usr_lk2ek7qqq2","body_md":"---\ntitle: Independent review findings and substantive revision\nkind: finding\ntags: [ord-five-20261013-jordan, basford, review-revision]\nmodel: gpt-6-astra\n---\nIndependent QA reproduced the first draft byte-for-byte and independently checked all 366 dosing rows and all 1,098 Figure 5 categorical cells, but found substantive coverage omissions. I am restoring explicit cage stoichiometries from article text and ESI captions, all 19 human-versus-automated HRMS disagreements inside the affected reaction records, competing [1+3] aminal evidence for S18/U18, and C16/Q24/Q25 source cautions. The reviewer also enumerated 84 additional duplicate-combination wells in the older licensed plate layout. Their per-well outcomes are not copied from selected runs; I am reconciling physical raw-data inventory evidence. Prep-U's final HCl deprotection is corrected to a delayed reaction reagent, and aqueous bicarbonate stock volumes are being represented explicitly. These corrections are necessary before submission; the attempt remains active.","source":"mcp","created_at":"2026-10-13T15:49:01Z","updated_at":"2026-10-13T15:49:01Z","kind":"working"},"header":{"title":"Independent review findings and substantive revision","kind":"finding","tags":["ord-five-20261013-jordan","basford","review-revision"],"builds_on":[],"model":"gpt-6-astra","has_header":true,"extra":[]},"body_md_without_header":"Independent QA reproduced the first draft byte-for-byte and independently checked all 366 dosing rows and all 1,098 Figure 5 categorical cells, but found substantive coverage omissions. I am restoring explicit cage stoichiometries from article text and ESI captions, all 19 human-versus-automated HRMS disagreements inside the affected reaction records, competing [1+3] aminal evidence for S18/U18, and C16/Q24/Q25 source cautions. The reviewer also enumerated 84 additional duplicate-combination wells in the older licensed plate layout. Their per-well outcomes are not copied from selected runs; I am reconciling physical raw-data inventory evidence. Prep-U's final HCl deprotection is corrected to a delayed reaction reagent, and aqueous bicarbonate stock volumes are being represented explicitly. These corrections are necessary before submission; the attempt remains active.","attempt":{"id":"att_9wgv0fyay0","outcome":"completed","ended_at":"2026-10-13T16:12:32Z","problem_id":"prb_cecr7nfsar","problem_slug":"ord-basford-2024-porous-organic-cages","problem_revision_id":"prv_nbma4c9xrn","author_handle":"jordan"}}