{"note":{"id":"nte_v60iq53fzs","attempt_id":"att_fwzkfjqh6e","author_user_id":"usr_lk2ek7qqq2","body_md":"---\ntitle: Draft dataset validated and frozen for independent review\nkind: result\ntags: [ord-five-20261013-jordan, ramirez, validation, phase-complete]\nmodel: Astra\n---\nBuilt 545 reactions with all 94 source fields preserved and companion mean/std/count provenance; 143 retained catalysts across six generations. Molecular identifiers for 20 species passed RDKit parse/formula audits. All 545 raw inlet-flow and time-on-stream means reproduce source means within 1.1e-14, and every analytical sample count matches. Official ord-schema 0.8.3 validation exited 0; API validation finds no errors. Remaining percentage warnings are true source values below 1%, not fractions, and are not rescaled. Sources archive contains all 117 checksummed author source files, scripts, README, exact validator output and audits.\n\nCoverage audit: author merge explicitly excludes three G2_NoCost XR4 rows. No author prose reason was found; extreme N2 outlet rates and non-closing carbon-selectivity sums support an analytical-anomaly inference. Excluded values/raw files remain in sources archive and a dedicated excluded-row CSV. G5 XD B has 96 valid GC records at 225/250/275°C plus one 300°C process row lacking a GC filename/result, so no 300°C outcomes were fabricated. Draft follows the author-merged selection, pending independent review of this decision. Gauge pressure is preserved exactly in pressure-control details and numeric metadata rather than assigned an assumed absolute offset. Time on stream is not mislabeled as reactor residence time.\n\nDataset SHA256 593d570bdb4ea8e1ae8a529d8f3a99af18f9c0d8da6f3744ca6842b23b7b1084; sources ZIP SHA256 6b504ad65f69c5a86dbf940b23fc459245b9ecad97edc7dc0921adc138dcc74a. Artifacts are frozen for an independent Codex/Astra review before any upload or submission.","source":"mcp","created_at":"2026-10-13T15:24:12Z","updated_at":"2026-10-13T15:24:12Z","kind":"working"},"header":{"title":"Draft dataset validated and frozen for independent review","kind":"result","tags":["ord-five-20261013-jordan","ramirez","validation","phase-complete"],"builds_on":[],"model":"Astra","has_header":true,"extra":[]},"body_md_without_header":"Built 545 reactions with all 94 source fields preserved and companion mean/std/count provenance; 143 retained catalysts across six generations. Molecular identifiers for 20 species passed RDKit parse/formula audits. All 545 raw inlet-flow and time-on-stream means reproduce source means within 1.1e-14, and every analytical sample count matches. Official ord-schema 0.8.3 validation exited 0; API validation finds no errors. Remaining percentage warnings are true source values below 1%, not fractions, and are not rescaled. Sources archive contains all 117 checksummed author source files, scripts, README, exact validator output and audits.\n\nCoverage audit: author merge explicitly excludes three G2_NoCost XR4 rows. No author prose reason was found; extreme N2 outlet rates and non-closing carbon-selectivity sums support an analytical-anomaly inference. Excluded values/raw files remain in sources archive and a dedicated excluded-row CSV. G5 XD B has 96 valid GC records at 225/250/275°C plus one 300°C process row lacking a GC filename/result, so no 300°C outcomes were fabricated. Draft follows the author-merged selection, pending independent review of this decision. Gauge pressure is preserved exactly in pressure-control details and numeric metadata rather than assigned an assumed absolute offset. Time on stream is not mislabeled as reactor residence time.\n\nDataset SHA256 593d570bdb4ea8e1ae8a529d8f3a99af18f9c0d8da6f3744ca6842b23b7b1084; sources ZIP SHA256 6b504ad65f69c5a86dbf940b23fc459245b9ecad97edc7dc0921adc138dcc74a. Artifacts are frozen for an independent Codex/Astra review before any upload or submission.","attempt":{"id":"att_fwzkfjqh6e","outcome":"completed","ended_at":"2026-10-13T15:48:36Z","problem_id":"prb_0nl8o27av8","problem_slug":"ord-ramirez-2024-co2-hydrogenation-hte","problem_revision_id":"prv_s17d3yhv0g","author_handle":"jordan"}}