{"revision":{"id":"prv_ybu7cjukn7","problem_id":"prb_7pc5i4u2ps","revision_number":1,"statement_md":"# Curate this paper into an ORD dataset\n\nBuild an Open Reaction Database (ORD) dataset of the reactions reported in:\n\n- **Paper:** Photocatalytic Aminative Suzuki–Miyaura C(sp2)–N–C(sp3) Cross-Coupling\n- **Authors:** Fujun Li, Yun Zou, Shuyang Liu et al.\n- **Published:** Org Lett, 2025-08-06\n- **DOI:** [10.1021/acs.orglett.5c02073](https://doi.org/10.1021/acs.orglett.5c02073)\n- **ORD wishlist card:** [open on GitHub](https://github.com/orgs/open-reaction-database/projects/11?pane=issue&itemId=126796329)\n\nThe reference input `card` holds these facts, the source-data locations and the notes below in machine-readable form.\n\n## Scope\n\nEvery reaction the paper reports with its data (the wishlist estimates about 432 reactions): inputs with amounts and roles, conditions, workups, outcomes and provenance, following the `ord-curation` Skill. Submit one ORD Dataset for the paper; if its data come from several screens or methods, keep them together and say so in the dataset description.\n\n## Source data\n\nSource: Li et al., Org. Lett. 2025, doi:10.1021/acs.orglett.5c02073. Photocatalytic aminative Suzuki-Miyaura C(sp2)-N-C(sp3) cross-coupling, about 432 reactions. The data is in the Supporting Information only as plate images and table images. Transcribe per-well outcomes and map them to conditions, then assign SMILES for all components from the structure drawings. Photochemical conditions (light source, wavelength, power, reactor) must be captured. The SI is ACS-hosted and not openly licensed. Cite it, but do not redistribute it.\n\nKnown locations:\n\n- [https://doi.org/10.1021/acs.orglett.5c02073](https://doi.org/10.1021/acs.orglett.5c02073): Org. Lett. article landing page and ACS-hosted SI PDF with plate and table images (license: ACS publisher terms (closed article))\n- [https://europepmc.org/article/MED/40770296](https://europepmc.org/article/MED/40770296): Europe PMC record (no open-access full text or SI available) (license: n/a)\n\n## Pitfalls\n\nOutcomes come from image transcription, so reviewers must spot-check values against the SI. The reaction is multi-component (aryl boronic acid, a nitrogen source and an alkyl partner), and plates may mix optimisation and scope, giving several templates or datasets. Illumination parameters are needed for ORD photochemistry fields.\n\n## Deliver\n\n- `dataset`: the ORD Dataset, compressed (`.binpb.gz`, `.pb.gz`, `.txtpb.gz`, `.pbtxt.gz` or `.parquet`), citing the DOI above in every reaction's provenance, with no dataset or reaction IDs.\n- `sources`: a `.zip` with a `README.md` (which tables or files each part came from, how structures were checked), the template and spreadsheet or the script or notebook that rebuild the dataset, and `validation.txt`, the output of ORD's validator (ord-schema 0.8.3) on the `dataset` file.\n\n## Before you start\n\nOpen the wishlist card. If it is no longer Available, someone has reserved or started it: coordinate with them or choose another paper. Get the source data only through legitimate channels (the publisher's Supporting Information, the repositories above, or the authors). Submitting the finished dataset to ORD, and ORD's separate Dataset Rewards program, follow ORD's own rules.\n","context_md":null,"benchmark":null,"verifier_contract_id":"vct_4t6ri8zibj","verifier_input_bindings":[{"key":"card","content_hash":"sha256:a99acc52c73951d7cb2fa5bddb010690353ecc6264deeb4269aaa946e9fc8664","size_bytes":2216,"media_type":"application/json","filename":"card.json"}],"skill_refs":[{"skill_version_id":"skv_k5sivlohu1","requirement":"required"}],"changelog_md":null,"created_by_user_id":"usr_llep2e937g","created_at":"2026-09-25T19:27:21Z","sealing":null}}