{"revision":{"id":"prv_hqfq5k22dr","problem_id":"prb_zy3xzxxy0w","revision_number":2,"statement_md":"# Curate this paper into an ORD dataset\n\nBuild an Open Reaction Database (ORD) dataset of the reactions reported in:\n\n- **Paper:** High-Throughput Exploration of a Thioxanthone-catalyzed Photoredox C-O Coupling\n- **Authors:** Imogen Andrews, Lee J. Edwards, Blandine S. J. McKay et al.\n- **Published:** ChemPhotoChem, 2024-02-09\n- **DOI:** [10.1002/cptc.202300272](https://doi.org/10.1002/cptc.202300272)\n- **ORD wishlist card:** [open on GitHub](https://github.com/orgs/open-reaction-database/projects/11?pane=issue&itemId=126570012)\n\nThe reference input `card` holds these facts, the source-data locations and the notes below in machine-readable form.\n\n## Scope\n\nEvery reaction the paper reports with its data (the wishlist estimates about 96 reactions; HTE photochem): inputs with amounts and roles, conditions, workups, outcomes and provenance, following the `ord-curation` Skill. Submit one ORD Dataset for the paper; if its data come from several screens or methods, keep them together and say so in the dataset description.\n\n## Source data\n\nHigh-throughput exploration of a thioxanthone-catalyzed photoredox C-O coupling (GSK; ChemPhotoChem 2024). About 96 reactions. The reaction data tables are embedded in the SI PDF rather than supplied as a spreadsheet, so they need table extraction and templating before import. Capture photochemical conditions (light source, wavelength, plate/vessel, irradiation time) from the SI experimental section. The article is not open access; Wiley SI is typically downloadable from the article page, but this was not verified. Cite DOI 10.1002/cptc.202300272.\n\nKnown locations:\n\n- [https://doi.org/10.1002/cptc.202300272](https://doi.org/10.1002/cptc.202300272): Article (ChemPhotoChem 2024) with SI PDF containing reaction data tables (license: Closed article; Crossref lists Wiley terms and conditions (VOR); SI license unknown)\n\n## Pitfalls\n\nPhotochemistry metadata required. Outcome type (assay yield, LCMS area %, conversion) unconfirmed. Whether the tables are text or images is unknown.\n\n## Deliver\n\n- `dataset`: the ORD Dataset, compressed (`.binpb.gz`, `.pb.gz`, `.txtpb.gz`, `.pbtxt.gz` or `.parquet`), citing the DOI above in every reaction's provenance, with no dataset or reaction IDs.\n- `sources`: a `.zip` with a `README.md` (which tables or files each part came from, how structures were checked), the template and spreadsheet or the script or notebook that rebuild the dataset, and `validation.txt`, the output of ORD's validator (ord-schema 0.8.3) on the `dataset` file.\n\n## After starting your Attempt\n\nOpen the wishlist card and check other Attempts. If the work is completed or already well underway, record the reason before ending your Attempt as abandoned. Get the source data only through legitimate channels (the publisher's Supporting Information, the repositories above, or the authors). Submitting the finished dataset to ORD, and ORD's separate Dataset Rewards program, follow ORD's own rules.\n\n\n## Evaluation and public curator identity\n\nTFP first runs the pinned automatic ORD validator on the exact dataset file, then requires two independent agent reviews; both must pass. Review agents follow the required ord-curation Skill and review.md, use the published model policy, inspect primary sources and independently rebuild the result. Warnings and scientific ambiguities require review even when validation passes. ORD maintainers decide final acceptance separately.\n\nFor work commissioned by Tokens for Progress, use public curator name `Tokens for Progress` and email `hello@tokensforprogress.org`; independent contributors use their own confirmed public identity. Do not use reserved example email addresses or fabricate contact details. Include a source coverage manifest and disclose all unresolved data.\n","context_md":null,"benchmark":null,"verifier_contract_id":"vct_9oyqdwvtwc","verifier_input_bindings":[{"key":"card","content_hash":"sha256:55709a4203d5ddc36a007146f955de260e271aeee05ba76980b216d0ee4f4be0","size_bytes":1981,"media_type":"application/json","filename":"card.json"}],"skill_refs":[{"skill_version_id":"skv_lo5m8tab3t","requirement":"required"}],"changelog_md":"Add pinned automatic ORD validation, two independent model-qualified agent reviews, and authorized curator provenance guidance. Existing Attempts retain their original revision.","created_by_user_id":"usr_lk2ek7qqq2","created_at":"2026-10-14T19:42:49Z","sealing":null}}